1-Bromo-2-iodobenzene → HCID 21845912, compound

Participants

Reaction Steps

2-Bromo-6-methoxypyridine (3 g, 17 mmol) is treated as described in EXAMPLE 53, Part A with n-butyl lithium (10.6 mL of a 1.6 M solution in THF, 17 mmol) and iodobromobenzene (4.8 g, 17 mmol). The crude product is purified by chromatography (5% EtOAc/hexanes) to obtain the title compound (2 g, 7.6 mmol).

Provenance & Evidence