HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → 1,1-Dimethyl-3-hydroxypiperidinium Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 3-Piperidinol, 1-methyl- | HCID 98016 | — |
| Product | 1,1-Dimethyl-3-hydroxypiperidinium Chloride | HCID 21247485 | — |
Reaction Steps
This compound was prepared by the procedure described for 2-[4-(N,N,N-trimethylammonium)phenyl]ethanol chloride. Typical reagent levels were as follows: 3-hydroxy-1-methylpiperidine (21.7 g, 0.188 mol), iodomethane (40.0 g, 0.280 mol) and methylene chloride (50 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04818426 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-0f06b4d483da430bbc56756d0f569330 |
| Source note | uspto-grants-1989_04 |