HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 21247553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 21247865 | HCID 21247865 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 21247553 | HCID 21247553 | — |
Reaction Steps
A mixture of 2.34 g of 2-phenyl-5-oxooctanoic acid, 0.3 g of NaBH4, 0.5 g of NaOH and 25 ml of methanol is boiled for 5 hours and worked up as usual. 2-Phenyl-5-hydroxyoctanoic acid is formed as an intermediate but is not isolated. 2-Oxo-3-phenyl-6-propyltetrahydropyran is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04818431 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-5ae1a70388764b41bace7306bc93e1e6 |
| Source note | uspto-grants-1989_04 |