HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4,5-Dihydroacephenanthrylene-6-carbaldehyde → 6-Acephenanthrylenecarbaldehyde
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4,5-Dihydroacephenanthrylene-6-carbaldehyde | HCID 14459539 | — |
| Lösungsmittel | Toluene hexane | HCID 21889329 | — |
| Produkt | 6-Acephenanthrylenecarbaldehyde | HCID 14371439 | 35,8% |
Reaktionsschritte
Using the dehydrogenation procedure outlined in Example 7B, 4,5-dihydroacephenanthrylene-6-carbaldehyde (J. P. Hoeffinger, P. Jacquignon, and N. P. Buu-Hoi, Bull. Soc. Chim. Fr. 974 (1970)) gave a 35.8% yield of 6-acephenanthrylenecarbaldehyde, mp 161°-163° (dec), (C,H), (PhCH3 /hexane).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04818443 |
| Quelldatensatz | uspto-grants-1989_04 |
| ORD ID | ord-f52c7d953e9c4056a68ab6681e106882 |
| Quellennotiz | uspto-grants-1989_04 |