1,2-Dibromoethane → HCID 21248442, compound

HRID 620089Notes

Reaction equation

HRID 620089 reaction equation
[C:1]([O:5][C:6]([NH:8][CH2:9][CH2:10][O:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][C:13]=1[OH:18])=[O:7])([CH3:4])([CH3:3])[CH3:2].[Br:19][CH2:20][CH2:21]Br>>[Br:19][CH2:20][CH2:21][O:18][C:13]1[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=1[O:11][CH2:10][CH2:9][NH:8][C:6]([O:5][C:1]([CH3:4])([CH3:2])[CH3:3])=[O:7]

Participants

3

Reactant 2

HCID 78391,2-DibromoethaneHCID 54205993HCID 54205993, compound

Product 1

HCID 21248442HCID 21248442, compound

Procedure

Reacting crude o-(2-tertiary butoxycarbonylaminoethoxy)-phenol with 1,2-dibromoethane analogously to Example 2 b yields 1-(2-bromoethoxy)-2-(2-tertiary butoxycarbonylaminoethoxy)-benzene, which has a melting point of 74°-75° (from isopropanol).

Sources & evidence

ORD record
ord-6a7ddfaa63464b7696dd5523bb094b5f
Source dataset
uspto-grants-1989_04
Patent number
US04818766

Reaction notes

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