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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 620090Generated: October 31, 2026

Benzyl 4-Hydroxybenzoate → HCID 14419466, compound

https://huagongshe.com/reaction/620090

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzyl 4-HydroxybenzoateHCID 7180—
ReactantPotassium CarbonateHCID 11430—
Reactant1,12-DibromododecaneHCID 18766—
SolventAcetoneHCID 180—
ProductHCID 14419466HCID 1441946682%

Reaction Steps

A solution of 150 mmol (49.2 g) of 1,12-dibromododecane, 50 mmol (10.6 g) of benzyl 4-hydroxybenzoate, and 0.3 mol (41.5 g) of potassium carbonate in 500 ml of acetone was refluxed for 6 hours. The reaction solution was then filtered and concentrated, and the resulting crude product was purified by column chromatography to obtain the objective ester compound of the following formula. (yield: 82%) ##STR34##

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04818807
Source datasetuspto-grants-1989_04
ORD IDord-a11a6b0fc5494f828fa0d4cbd32d0c7f
Source noteuspto-grants-1989_04