HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl 4-Hydroxybenzoate → HCID 14419466, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl 4-Hydroxybenzoate | HCID 7180 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1,12-Dibromododecane | HCID 18766 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 14419466 | HCID 14419466 | 82% |
Reaction Steps
A solution of 150 mmol (49.2 g) of 1,12-dibromododecane, 50 mmol (10.6 g) of benzyl 4-hydroxybenzoate, and 0.3 mol (41.5 g) of potassium carbonate in 500 ml of acetone was refluxed for 6 hours. The reaction solution was then filtered and concentrated, and the resulting crude product was purified by column chromatography to obtain the objective ester compound of the following formula. (yield: 82%) ##STR34##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04818807 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-a11a6b0fc5494f828fa0d4cbd32d0c7f |
| Source note | uspto-grants-1989_04 |