HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13280856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | HCID 19818641 | HCID 19818641 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 13280856 | HCID 13280856 | — |
Reaction Steps
5 g of boron tribromide are added dropwise to a solution, cooled to -78° C., of 2 g of methyl N-(3-methoxyphenyl)-oxamate in 20 ml of methylene chloride in the course of 5 minutes. The mixture is stirred at room temperature for 5 hours, 5 ml of water are added, with cooling, and the organic phase is separated off. Drying over sodium sulfate and evaporation gives methyl N-(3-hydroxyphenyl)-oxamate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820726 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-77e49e6bf1194c2b9e330ac2fc845f5a |
| Source note | uspto-grants-1989_04 |