HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21246152, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | Sodium ethoxide | HCID 2723922 | — |
| Reactant | HCID 21246151 | HCID 21246151 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 21246152 | HCID 21246152 | — |
Reaction Steps
A solution of ethyl 3-(2-allyloxyphenyl)-4,4-diethoxy-2-ethoxycarbonylbutanoate (described in Example 1(i)), in ether is treated with sodium ethoxide and subsequently with methyl iodide to give ethyl 3-(2-allyloxyphenyl)-4,4-diethoxy-2-ethoxycarbonyl-2-methylbutanoate, which is subsequently reacted in a manner similar to that described in Example 1(i) to give 4-(2-allyloxyphenyl)-5-ethoxy-3-methyl-2-oxotetrahydrofuran.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820819 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-4b898c651cd64e31be952f3bb6a1d088 |
| Source note | uspto-grants-1989_04 |