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HRID620459

反应详情

EQUATION

反应方程式

HRID 620459 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccc(Cl)cc1
HCID7474

1-Chloro-4-nitrobenzene

C6H4ClNO2

结构：CC(C)C(O)C(C)(C)CO
HCID8946

2,2,4-Trimethyl-1,3-pentanediol

C8H18O2

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

PRODUCTS

生成物

1
结构：CC(C)C(Oc1ccc([N+](=O)[O-])cc1)C(C)(C)COc1ccc([N+](=O)[O-])cc1
HCID19860678

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CS(C)=O
溶剂HCID679

Dimethyl sulfoxide

C2H6OS

PROCEDURE

实验过程

146 g (1 mol) 2,2,4-trimethyl-1,3-dihydroxypentane, 346.5 g (2.2 mols) 4-nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted using the same procedure described in Example 1 in 600 ml DMSO.

WORKUP

后处理

  1. customwere reacted