HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylene Glycol → 1,1'-[Ethane-1,2-diylbis(oxy)]bis(4-nitrobenzene)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | 1-Chloro-4-nitrobenzene | HCID 7474 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | 1,1'-[Ethane-1,2-diylbis(oxy)]bis(4-nitrobenzene) | HCID 270647 | — |
Reaction Steps
62 g (1 mol) ethylene glycol, 346.5 g (2.2 mols) 4-nitrochlorobenzene and 140 g powdered sodium hydroxide were reacted following the procedure described in Example 1 in 600 ml DMSO.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04820866 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-334e4f855d35439fade44388f57b82b1 |
| Source note | uspto-grants-1989_04 |