4-Chlorobenzoyl chloride → HCID 909539, compound

HRID 621409Notes

Reaction equation

HRID 621409 reaction equation
[C:1]([O:5][CH3:6])(=[O:4])[NH:2][NH2:3].[Cl:7][C:8]1[CH:16]=[CH:15][C:11]([C:12](Cl)=[O:13])=[CH:10][CH:9]=1>>[Cl:7][C:8]1[CH:16]=[CH:15][C:11]([C:12]([NH:3][NH:2][C:1]([O:5][CH3:6])=[O:4])=[O:13])=[CH:10][CH:9]=1

Participants

3

Reactant 2

HCID 85014-Chlorobenzoyl chlorideHCID 80519Methyl carbazate

Product 1

HCID 909539HCID 909539, compoundYield 81.5%

Procedure

36.0 g. (0.4 moles) of methyl carbazate and 70.0 g. (0.4 moles) of p-chloro-benzoyl chloride are reacted in an analogous manner to Example 2. Thus 74.5 g. of the desired compound are obtained, yield 81.5%, m.p.: 160° C.

Sources & evidence

ORD record
ord-c09a8416fd75466381794a45272167e1
Source dataset
uspto-grants-1989_04
Patent number
US04824670

Reaction notes

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