Oxygen → 3-Ethyloxetane-3-carboxylic acid

HRID 621752Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 621752
[O:1]=O.[CH2:3]([C:5]1([CH2:9][OH:10])[CH2:8][O:7][CH2:6]1)[CH3:4]>>[CH2:3]([C:5]1([C:9]([OH:1])=[O:10])[CH2:8][O:7][CH2:6]1)[CH3:4]

Komponenten

3

Edukt 2

HCID 977OxygenHCID 76444Oxt-101

Produkt 1

HCID 140289983-Ethyloxetane-3-carboxylic acidAusbeute 86,2 %

Versuchsvorschrift

The procedure as in Example 10 is carried, but at an oxidation temperature of 50° C. After 2 hours, 0.9 mol of oxygen has been taken up per mol of 3-ethyl-3-hydroxymethyl-oxetane. After working up, 3-ethyl-oxetane-3-carboxylic acid is obtained in a yield of 86.2% of theory.

Aufarbeitung

  1. customat an oxidation temperature of 50° C

Quellen und Nachweise

ORD-Eintrag
ord-a4e51c8fe0644a3fbba3ffc860351c44
Quelldatensatz
uspto-grants-1989_04
Patentnummer
US04824975

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