Thionyl Chloride → HCID 13355212, compound

HRID 621759Notes

Reaction equation

[CH3:1][C:2]([CH3:18])([O:4][C:5]([NH:7][CH:8]1[CH2:12][O:11][C:10](O)([C:13]([O:15][CH3:16])=[O:14])[CH2:9]1)=[O:6])[CH3:3].S(Cl)(Cl)=O>>[CH3:3][C:2]([CH3:18])([O:4][C:5]([NH:7][CH:8]1[CH2:12][O:11][C:10]([C:13]([O:15][CH3:16])=[O:14])=[CH:9]1)=[O:6])[CH3:1]

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 13355210HCID 13355210, compound

Product 1

HCID 13355212HCID 13355212, compound

Procedure

The process of claim 1, wherein in step (g) methyl 4-[[(1,1-dimethylethoxy)-carbonyl]amino]-2-hydroxytetrahydrofuran-2-carboxylate is reacted with thionyl chloride to produce methyl 4-[[(1,1-dimethylethoxy)carbonyl]amino]-4,5-dihydro-2-furan-carboxylate.

Sources & evidence

ORD record: ord-d3b615914d6847e2b44c43b41a8930a6
Source dataset: uspto-grants-1989_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04824974

Reaction notes

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