HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl oxalate → HCID 54697154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl oxalate | HCID 11120 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 21243565 | HCID 21243565 | — |
| Product | HCID 54697154 | HCID 54697154 | 43.4% |
Reaction Steps
Prepared by the method described in Example 15 from dimethyl α-phenyl-thiodiglycolate (9.0 g, 35 mmoles), dimethyl oxalate (6.1 g, 52 mmoles) and sodium (2.5 g, 109 mmoles). The product is obtained as a beige powder (3.8 g); mp 143°-144° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04824958 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-d64cd0a4acb545df827deb0eeeea883f |
| Source note | uspto-grants-1989_04 |