HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 23037411, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | HCID 14390379 | HCID 14390379 | — |
| Reactant | Isopropanol hydrochloride | HCID 21912024 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 23037411 | HCID 23037411 | — |
Reaction Steps
A solution of 2-(4-chlorophenyl)-N-[3-(dimethylamino)phenyl]-3H-imidazo[4,5-b]pyridine-3-acetamide in hot isopropyl alcohol was acidified with hydrogen chloride/isopropyl alcohol. Isopropyl ether was added to the cloud point. Upon cooling to room temperature, solid fomred which was collected by filtration, rinsed with isopropyl ether, and dried under high vacuum at 50° C. overnight to give 1.9 g of title compound, mp 166°-170° C. (shrinks), 183°-187° C. (melts).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04824951 |
| Source dataset | uspto-grants-1989_04 |
| ORD ID | ord-e807c74ae9b043d1b59fc495f15fe59c |
| Source note | uspto-grants-1989_04 |