Titanium Tetrachloride → HCID 86698323, compound

HRID 622062Notes

Reaction equation

HRID 622062 reaction equation
[Al+3:1].[Cl-:2].[Cl-].[Cl-].[Cl:5][Ti:6]([Cl:9])([Cl:8])[Cl:7]>O>[Al+3:1].[Cl-:5].[Cl-:2].[Cl-:5].[Cl:5][Ti:6]([Cl:9])([Cl:8])[Cl:7]

Participants

4

Reactant 2

HCID 24193Titanium Tetrachloride3×HCID 6451240Aluminum(III) Chloride2×

Product 1

HCID 86698323HCID 86698323, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

An acidic solution was made by diluting 25 liters of a 28 wt. % AlCl3 solution to 60 liters total volume with water. In addition, a TiCl4 solution was made by adding 3200 ml of TiCl4 to 4,000 ml of water to obtain a clear solution. The TiCl4 solution was added to the previously prepared AlCl3 solution to form an AlCl3 -TiCl4 solution. A base solution was made by dissolving 9,000 g of NaOH in 60 liters of water. Then the following precipitation reaction was carried out:

Workup

  1. customto obtain a clear solution

Sources & evidence

ORD record
ord-674108934ff14b54af7f4bad51238138
Source dataset
uspto-grants-1988_09
Patent number
US04769079

Reaction notes

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