Morpholine, 4-(1-cyclohexen-1-yl)- → HCID 13770134, compound

HRID 622085Notes

Reaction equation

HRID 622085 reaction equation
[N+:1]([C:4]([C:16](=[O:18])[CH3:17])=[CH:5][C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=1[C:12]([F:15])([F:14])[F:13])([O-:3])=[O:2].[O:19]1[CH2:24][CH2:23][N:22]([C:25]2[CH2:30][CH2:29][CH2:28][CH2:27][CH:26]=2)[CH2:21][CH2:20]1>C(O)C>[CH3:17][C:16]1[O:18][C:25]2([N:22]3[CH2:23][CH2:24][O:19][CH2:20][CH2:21]3)[CH:30]([CH:5]([C:6]3[CH:11]=[CH:10][CH:9]=[CH:8][C:7]=3[C:12]([F:13])([F:14])[F:15])[C:4]=1[N+:1]([O-:3])=[O:2])[CH2:29][CH2:28][CH2:27][CH2:26]2

Participants

4

Reactant 2

HCID 69589Morpholine, 4-(1-cyclohexen-1-yl)-HCID 53729837HCID 53729837, compound

Product 1

HCID 13770134HCID 13770134, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

10.4 g (40 mmol) of 2-nitro-1-(2-trifluoromethylphenyl)-but-1-en-3-one and 6.7 g (40 mmol) of 1-morpholinocyclohexene are brought together in 20 ml of ethanol at room temperature. An exothermic reaction takes place and after a short time the product crystallizes in pale yellow crystals as an isomer mixture.

Workup

  1. customAn exothermic reaction
  2. customafter a short time the product crystallizes in pale yellow crystals as an isomer mixture

Sources & evidence

ORD record
ord-4eff4159e46c469aa3645e04ea5cd15f
Source dataset
uspto-grants-1988_09
Patent number
US04769375

Reaction notes

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