HuagongsheHuagongshe Chemistry Print Report · For research reference only
11-Bromo-1-undecanol → 11-Bromoundecanal
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 11-Bromo-1-undecanol | HCID 74163 | — |
| Reactant | HCID 178418287 | HCID 178418287 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 11-Bromoundecanal | HCID 12479241 | — |
Reaction Steps
1-Bromo-11-hydroxyundecane (5 g, 20 mmoles) dissolved in methylene chloride (30 ml) was added to a suspension of pyridinium chlorochromate (6.4 g, 30 mmoles) in methylene chloride (25 ml) and stirred for 2 hours. The mixture was diluted with ether, filtered and concentrated in vacuo to afford 1-bromo-11-oxoundecane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04769386 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-db995520fdf843699ff5858c4e63df22 |
| Source note | uspto-grants-1988_09 |