HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → Methyl 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-2,2-dimethylhexanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2',4'-Dihydroxy-3'-propylacetophenone | HCID 2775198 | — |
| Reactant | Methyl 6-bromo-2,2-dimethylhexanoate | HCID 15666632 | — |
| Product | Methyl 6-(4-acetyl-3-hydroxy-2-propylphenoxy)-2,2-dimethylhexanoate | HCID 21294040 | — |
Reaction Steps
Following the procedure of Example 15, 2.5 g. of methyl 6-bromo-2,2-dimethylhexanoate, 1.46 g. of potassium carbonate, a catalytic amount of potassium iodide, and 2.14 g. of 2,4-dihydroxy-3-propylacetophenone were reacted to give 2.96 g. of the title product as a brown oil. IR, NMR.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04769482 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-45b7d15501244053b12a2f51dd4290d0 |
| Source note | uspto-grants-1988_09 |