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HRID622324

反应详情

EQUATION

反应方程式

HRID 622324 的结构方程式

REACTANTS

反应物

2
结构：O=C1c2cccc([N+](=O)[O-])c2C(=O)C2CC=CCC12
HCID10868940

未命名化合物

结构：CC1=C(C)CC2C(=O)c3c(cccc3[N+](=O)[O-])C(=O)C2C1
HCID21292554

1,4,4a,9a-Tetrahydro-2,3-dimethyl-5-nitro-9,10-anthracenedione

C16H15NO4

PRODUCTS

生成物

1
结构：Cc1cc2c(cc1C)C(=O)c1c(N)cccc1C2=O
HCID21292553

1-Amino-6,7-dimethylanthracene-9,10-dione

C16H13NO2

收率 99%

PROCEDURE

实验过程

The process of Example 1 is repeated, replacing 64.3 parts of 5-nitro-1,4,4a,9a-tetrahydroanthraquinone by 71.3 parts of 5-nitro-2,3-dimethyl-1,4,4a,9a-tetrahydroanthraquinone (obtained from 1-nitronaphthoquinone and 2,3-dimethyl-1,4-butadiene by Diels-Alder reaction), to give 61.9 parts of 1-amino-6,7-dimethylanthraquinone in 99% purity, corresponding to a yield of 99% of theory.