HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diphosgene → Isatoic Anhydride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diphosgene | HCID 10426 | — |
| Reactant | Anthranilic acid, hydrochloride | HCID 74985 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Isatoic Anhydride | HCID 8359 | — |
Reaction Steps
7.5 g of 2-amino benzoic acid hydrochloride was mixed with 10 ml of diphosgene and the mixture was stirred in 150 ml of dioxane for 40 minutes at reflux. The resulting mixture was cooled and filtered. Yield: 5.7 g of title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04771051 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-e86f8072299c45e784bcf15e86d0aed2 |
| Source note | uspto-grants-1988_09 |