Sodium borohydride → HCID 14254894, compound

HRID 622643Notes

Reaction equation

HRID 622643 reaction equation
C[O:2][C:3]([CH:5]1[N:9]([CH2:10][C:11]#[CH:12])[C:8](=[O:13])[CH2:7][CH2:6]1)=O.[BH4-].[Na+]>C(O)C>[OH:2][CH2:3][CH:5]1[N:9]([CH2:10][C:11]#[CH:12])[C:8](=[O:13])[CH2:7][CH2:6]1

Participants

4

Reactant 2

HCID 4311764Sodium borohydrideHCID 14254893HCID 14254893, compound

Product 1

HCID 14254894HCID 14254894, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

To an ice-water chilled solution of 6.42 g of 5-methoxycarbonyl-1-(2-propynyl)-2-pyrrolidinone in absolute ethanol (60 ml), 1.55 g of powdered sodium borohydride was added. The mixture was stirred overnight at ambient temperature.

Sources & evidence

ORD record
ord-bf4afd00c8a14d1aa9c65702c8e5f031
Source dataset
uspto-grants-1988_09
Patent number
US04772601

Reaction notes

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