HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dimethylpiperazine → N-alpha-chloroethoxycarbonyl N'-methyl piperazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dimethylpiperazine | HCID 7818 | — |
| Reactant | 1-Chloroethyl chloroformate | HCID 521305 | — |
| Product | N-alpha-chloroethoxycarbonyl N'-methyl piperazine | HCID 21291932 | — |
Reaction Steps
In a similar manner, N,N'-di-methylpiperazine is reacted with α-chloroethyl chloroformate (ACE-Cl) to give the intermediate N-α-chloroethoxycarbonyl N'-methyl piperazine, which is then dehydrohalogenated as in Example 21b to give N-(vinyloxycarbonyl)N'-methylpiperazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04772695 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-fe6304217b9245949ae64174996e8177 |
| Source note | uspto-grants-1988_09 |