HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 23037389, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 14390216 | HCID 14390216 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 23037389 | HCID 23037389 | — |
Reaction Steps
Solid 2-(4-chlorophenyl)-N-(3-pyridinyl)-3H-imidazo[4,5-b]pyridine-3-acetamide (0.50 g) was dissolved in isopropyl alcohol and acidified with excess ethereal hydrogen chloride to produce a crystalline precipitate. The solid was collected, washed with ether, and dried under high vacuum at room temperature overnight to give 0.58 g (91%), mp 189°-91° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04772600 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-1b9581a628044467aa8a9b254abccf2b |
| Source note | uspto-grants-1988_09 |