HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclohexane → Spiro[cyclohexane-1,9'-fluorene]
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclohexane | HCID 8078 | — |
| Catalyst | HCID 178503044 | HCID 178503044 | — |
| Product | Spiro[cyclohexane-1,9'-fluorene] | HCID 12861606 | — |
Reaction Steps
110 g of spiro[cyclohexane-1,9'-fluorene] obtained in the above (1), 100 ml of cyclohexane solvent and 20 g of 5% ruthenium-carbon catalyst (manufactured by Japan Engelhard Co.) were charged in an autoclave of 1 liter and hydrogenation was effected with a hydrogen pressure of 80 kg/cm2G at 170° C. for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04774013 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-898e96dc55a24a45876203d87c37ab65 |
| Source note | uspto-grants-1988_09 |