HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzophenone → 4,4'-(1,3-Dioxolane-2,2-diyl)diphenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzophenone | HCID 3102 | — |
| Reactant | 4,4'-Dihydroxybenzophenone | HCID 69150 | — |
| Reactant | 2,2-Diphenyl-1,3-dioxolane | HCID 283230 | — |
| Product | 4,4'-(1,3-Dioxolane-2,2-diyl)diphenol | HCID 14765955 | — |
Reaction Steps
The preparation of 2,2-diphenyl-1,3-dioxolane from benzopheone under similar conditions is reported to give over 80% yield in only 5 hours reaction time, [M. Sulzbacher et al., J. Amer. Chem. Soc., 70, 2827 (1948)]. It is readily apparent that the synthesis of the ketal of 4,4'-dihydroxybenzophenone is accomplished less advantageously than the corresponding ketal of benzophenone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04774344 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-7ffac1569c974ecc9f5d1d93a94fc168 |
| Source note | uspto-grants-1988_09 |