HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,2-Dichloroethane → 1,1-Dichloroethane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,2-Dichloroethane | HCID 11 | — |
| Reactant | Ethylene | HCID 6325 | — |
| Reactant | Chlorine | HCID 24526 | — |
| Product | 1,1-Dichloroethane | HCID 6365 | — |
| Product | 1,1,2-Trichloroethane | HCID 6574 | — |
Reaction Steps
The procedure was as in Example 1 but 2072 g 1,2-dichloroethane containing 1.6 g dissolved FeCl3 was introduced into the reactor. The solution contained 0.076 weight % FeCl3, determined colorimetrically. The quantities of ethylene and chlorine introduced in the presence of air underwent reaction inside the reactor to give crude dichloroethane containing 0.18 weight % 1,1,2-trichloroethane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04774373 |
| Source dataset | uspto-grants-1988_09 |
| ORD ID | ord-df26eb28ea1b4d138e706d84fca5ee55 |
| Source note | uspto-grants-1988_09 |