HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propionyl chloride → HCID 67510107, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propionyl chloride | HCID 62324 | — |
| Reactant | HCID 67509572 | HCID 67509572 | — |
| Product | HCID 67510107 | HCID 67510107 | 18% |
Reaction Steps
The title compound is prepared in 18% yield (5.1 mg) from 6-amino-N-(1-(6-(2,2,2-trifluoroethoxy)pyridin-3-yl)ethyl)picolinamide (25 mg, 0.073 mmol, Step-1, single enantiomer) and propionyl chloride (24 mg, 0.26 mmol) by the similar manner in Step-2 of Example-8.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09302991B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-3a96b3c103ac4982b4f07216f819cc7e |
| Source note | uspto-grants-2016_04 |