HCID 68283326, compound → HCID 86704218, compound

HRID 624061Notes

Reaction equation

HRID 624061 reaction equation
[CH3:1][S:2]([O:5][CH2:6][CH2:7][CH2:8][C:9]1[N:14]=[C:13]([O:15][CH3:16])[CH:12]=[C:11]([O:17][CH3:18])[N:10]=1)(=[O:4])=[O:3].[CH2:19](OC1C=C(OC)N=C(CCCO)N=1)C>>[CH3:1][S:2]([O:5][CH2:6][CH2:7][CH2:8][C:9]1[N:14]=[C:13]([O:15][CH2:16][CH3:19])[CH:12]=[C:11]([O:17][CH3:18])[N:10]=1)(=[O:3])=[O:4]

Participants

3

Reactant 2

HCID 68283326HCID 68283326, compoundHCID 86704217HCID 86704217, compound

Product 1

HCID 86704218HCID 86704218, compound

Procedure

The title compound was synthesized according to the procedure described for 3-(4,6-dimethoxypyrimidin-2-yl)propyl methanesulfonate (step 4), starting from 3-(4-ethoxy-6-methoxypyrimidin-2-yl)propan-1-ol. LC-MS conditions B: tR=0.68 min, [M+H]+=291.08.

Sources & evidence

ORD record
ord-9f1843f91ff9448498b7ee869d04071b
Source dataset
uspto-grants-2016_04
Patent number
US09303023B2

Reaction notes

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