HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → HCID 57509968, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | HCID 57509898 | HCID 57509898 | — |
| Reactant | HCID 68754543 | HCID 68754543 | — |
| Product | HCID 57509968 | HCID 57509968 | — |
Reaction Steps
The title compound was prepared as described in Example 278, substituting benzoyl chloride for acetyl chloride and N-(isoindolin-5-yl)isoindoline-2-carboxamide for 5-amino-N-(4-(propylcarbamoyl)phenyl)isoindoline-2-carboxamide. 1H NMR (400 MHz, DMSO-d6) δ ppm 8.40 (d, J=8.8 Hz, 1H), 7.59-7.67 (m, 3H), 7.11-7.52 (m, 9H), 4.68-4.84 (m, 8H); MS (ESI(+)) m/e 384 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09302989B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-3762b0cfd8fd4db282c91e45ddf546a5 |
| Source note | uspto-grants-2016_04 |