HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Furancarboxaldehyde, tetrahydro- → HCID 57510514, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Furancarboxaldehyde, tetrahydro- | HCID 157568 | — |
| Reactant | HCID 68753566 | HCID 68753566 | — |
| Product | HCID 57510514 | HCID 57510514 | — |
Reaction Steps
The title compound was prepared as described in Example 926, substituting N-(4-(piperidin-4-yl)phenyl)-1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxamide for N-(4-(1,2,3,6-tetrahydropyridin-4-yl)phenyl)-1H-pyrrolo[3,4-c]pyridine-2(3H)-carboxamide and tetrahydrofuran-3-carbaldehyde for isobutraldehyde. 1H NMR (400 MHz, DMSO-d6) δ ppm 8.60 (s, 1H), 8.50 (d, J=5.0 Hz, 1H), 8.33 (s, 1H), 7.44 (m, 3H), 7.13 (m, 2H), 4.78 (m, 4H), 3.71 (m, 2H), 3.61 (q, J=7.6 Hz, 1H), 3.36 (m, 2H), 2.96 (m, 2H), 2.40 (m, 1H), 2.27 (m, 2H), 96 (m, 3H), 1.72 (m, 2H), 1.66-1.46 (m, 3H); MS (ESI(+)) m/e 407 (M+H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09302989B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-4da220b340a84a79b7fb64851d944351 |
| Source note | uspto-grants-2016_04 |