HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovaleric Acid → HCID 57510952, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovaleric Acid | HCID 10430 | — |
| Reactant | 3-Phenylpropylamine | HCID 16259 | — |
| Reactant | HCID 62230337 | HCID 62230337 | — |
| Product | HCID 57510952 | HCID 57510952 | — |
Reaction Steps
The title compound was prepared as described in Example 1C, substituting N-(4-(2-aminoethyl)phenyl)isoindoline-2-carboxamide for 3-phenylpropan-1-amine and 3-methylbutanoic acid for 4-(isoindoline-2-carboxamido)benzoic acid. 1H NMR (400 MHz, DMSO-d6, Temp=90° C.) δ 7.50-7.40 (m, 2H), 7.40-7.24 (m, 4H), 7.13-7.02 (m, 2H), 4.76 (s, 4H), 2.68 (t, J=7.3 Hz, 2H), 2.07-1.84 (m, 3H), 0.95-0.76 (m, 6H). MS (ESI (+)) m/e 366 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09302989B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-df8d58e0be554ecbbe72dd23cc27ed1e |
| Source note | uspto-grants-2016_04 |