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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 624265Generated: October 31, 2026

Isovaleric Acid → HCID 57510952, compound

https://huagongshe.com/reaction/624265

Reaction equation

Participants

RoleNameHCIDCharge
ReactantIsovaleric AcidHCID 10430—
Reactant3-PhenylpropylamineHCID 16259—
ReactantHCID 62230337HCID 62230337—
ProductHCID 57510952HCID 57510952—

Reaction Steps

The title compound was prepared as described in Example 1C, substituting N-(4-(2-aminoethyl)phenyl)isoindoline-2-carboxamide for 3-phenylpropan-1-amine and 3-methylbutanoic acid for 4-(isoindoline-2-carboxamido)benzoic acid. 1H NMR (400 MHz, DMSO-d6, Temp=90° C.) δ 7.50-7.40 (m, 2H), 7.40-7.24 (m, 4H), 7.13-7.02 (m, 2H), 4.76 (s, 4H), 2.68 (t, J=7.3 Hz, 2H), 2.07-1.84 (m, 3H), 0.95-0.76 (m, 6H). MS (ESI (+)) m/e 366 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09302989B2
Source datasetuspto-grants-2016_04
ORD IDord-df8d58e0be554ecbbe72dd23cc27ed1e
Source noteuspto-grants-2016_04