HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Prolinamide → HCID 90203995, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Prolinamide | HCID 111306 | — |
| Reactant | 5-Cyclopropyl-6-cyclopropylmethoxy-pyridine-2-carboxylic acid | HCID 71087346 | — |
| Product | HCID 90203995 | HCID 90203995 | — |
Reaction Steps
The title compound was synthesized in analogy to Example 47 b, using 5-cyclopropyl-6-cyclopropylmethoxy-pyridine-2-carboxylic acid (Example 3 c, 40 mg, 171 μmol) and (2S)-2-pyrrolidinecarboxamide (CAN 7531-52-4; 21.5 mg, 189 μmol) as starting materials and isolated (49 mg, 87%) as white solid; LC-MS (UV peak area, ESI) 100%, 330.1818 [MH+].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303012B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-ef9398d0570745ada74a40f7f21f6631 |
| Source note | uspto-grants-2016_04 |