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HRID624953

反应详情

EQUATION

反应方程式

HRID 624953 的结构方程式

REACTANTS

反应物

2
结构：NC(=O)C1CCCCN1
HCID140623

piperidine-2-carboxamide

C6H12N2O

结构：O=C(O)c1ccc(C2CC2)c(OCC2CC2)n1
HCID71087346

未命名化合物

PRODUCTS

生成物

1
结构：NC(=O)C1CCCCN1C(=O)c1ccc(C2CC2)c(OCC2CC2)n1
HCID76282619

未命名化合物

PROCEDURE

实验过程

The title compound was synthesized in analogy to Example 47 b, using 5-cyclopropyl-6-cyclopropylmethoxy-pyridine-2-carboxylic acid (Example 3 c, 100 mg, 429 μmol) and 2-piperidinecarboxamide (CAN 19889-77-1, 60.4 mg, 472 μmol) as starting materials and isolated (135 mg, 92%) as white solid; LC-MS (UV peak area, ESI) 100%, 344.1972 [MH+].

WORKUP

后处理

  1. customisolated (135 mg, 92%) as white solid