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HRID625006

反应详情

EQUATION

反应方程式

HRID 625006 的结构方程式

REACTANTS

反应物

2
结构：N
HCID222

Ammonia gas

H3N

结构：CC(C)(C)OC(=O)N1CC2(CC2)CC1C(=O)O
HCID66620594

5-Azaspiro[2.4]heptane-5,6-dicarboxylic acid, 5-(1,1-dimethylethyl) ester

C12H19NO4

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CC2(CC2)CC1C(N)=O
HCID90203364

未命名化合物

收率 78%

PROCEDURE

实验过程

In analogy to the procedure described in Example 127 c), 5-(tert-butoxycarbonyl)-5-azaspiro[2.4]heptane-6-carboxylic acid (CAN 1454843-77-6, 112 mg, 464 μmol) was condensed with ammonia to give the title compound (87 mg, 78%) as colorless liquid, MS (EI): m/e=240.0 [M+].