HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acrylonitrile → 3-Cyclohexene-1-carbonitrile, 3,4-dimethyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | 2,3-Dimethyl-1,3-butadiene | HCID 10566 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-Cyclohexene-1-carbonitrile, 3,4-dimethyl- | HCID 11137219 | 87% |
Reaction Steps
A solution of acrylonitrile (1 eq.) and 2,3-dimethylbuta-1,3-diene (1.1 eq.) in toluene (2M) was pumped through a heated coil reactor at 240° C. with a residence time of 10 minutes. The resulting mixture was concentrated under reduced pressure and yielded the product as colorless oil (87% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09303232B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-b54ff47562704e93b1e2067e66822843 |
| Source note | uspto-grants-2016_04 |