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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 625163Generated: October 25, 2026

Acrylonitrile → 3-Cyclohexene-1-carbonitrile, 3,4-dimethyl-

https://huagongshe.com/reaction/625163

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcrylonitrileHCID 7855—
Reactant2,3-Dimethyl-1,3-butadieneHCID 10566—
SolventTolueneHCID 1140—
Product3-Cyclohexene-1-carbonitrile, 3,4-dimethyl-HCID 1113721987%

Reaction Steps

A solution of acrylonitrile (1 eq.) and 2,3-dimethylbuta-1,3-diene (1.1 eq.) in toluene (2M) was pumped through a heated coil reactor at 240° C. with a residence time of 10 minutes. The resulting mixture was concentrated under reduced pressure and yielded the product as colorless oil (87% yield).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09303232B2
Source datasetuspto-grants-2016_04
ORD IDord-b54ff47562704e93b1e2067e66822843
Source noteuspto-grants-2016_04