Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Toluene | HCID 1140 | — |
| Reactant | L-Pyroglutamic Acid | HCID 7405 | — |
| Reactant | Benzoyl chloride | HCID 7412 | — |
| Reactant | HCID 71503470 | HCID 71503470 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 71503471 | HCID 71503471 | — |
Reaction Steps
Nucleoside 102-U (3.01 g, 5.50 mmol) was coevaporated with an. toluene (15 mL). The resulting residue was dissolved in an. DCM (150 mL) along with an. Pyr. (4.4 mL) and the mixture was cooled to −70° C. Benzoyl chloride (700 μL, 6 mmol) was slowly added to the reaction mixture and stirred for 1 h at −70° C. EtOH (5 mL) was added to the solution and subsequently allowed to reach rt. The reaction mixture was washed with sat. aq. NaHCO3 (3×100 mL) and brine (100 mL). The combined aqueous phase was back extracted with CH2Cl2 (100 mL). The organic phases were combined and evaporated. The resulting residue was purified by column chromatography (3.5% MeOH in DCM) affording the product 103-U as a white foam after evaporation of the solvents.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US09303260B2 |
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| Source dataset | uspto-grants-2016_04 |
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| ORD ID | ord-97504f658add4de9ac41c1f3ac536245 |
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| Source note | uspto-grants-2016_04 |
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