Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methane | HCID 297 | — |
| Reactant | Biphenyl | HCID 7095 | — |
| Reactant | O-Phenylenediamine | HCID 7243 | — |
| Reactant | N-ethyl-2-pyrrolidone | HCID 17595 | — |
| Product | Biphenyl | HCID 7095 | — |
| Product | Phenylenediamine carbon black | HCID 131733384 | — |
Reaction Steps
More specifically, an intermediate transfer coating dispersion was prepared by providing a mixture of Special Carbon Black 4, available from Orion Chemicals, N-ethyl-2-pyrrolidone (NMP) about 18 weight percent of solids, the polyamic acid of biphenyl tetracarboxylicdianhydride/phenylenediamine, and the leveling agent NOVEC™ FC-4432, a fluoro surfactant available from 3M, and which mixture was stirred and subjected to ball milling with 2 millimeter stainless steel shots via an Attritor grinding mill for 18 hours. There resulted a coating dispersion of the polyamic acid of biphenyl tetracarboxylicdianhydride/phenylenediamine/carbon black/leveling agent dispersed in NMP, where the weight ratio of polyamic acid of biphenyl tetracarboxylicdianhydride/phenylenediamine/carbon black/leveling agent was 88.8/11/0.2, and which dispersion was filtered with a 20 micron Nylon cloth filter.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US09304448B2 |
|---|
| Source dataset | uspto-grants-2016_04 |
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| ORD ID | ord-d0039feb445846f99886708563977f43 |
|---|
| Source note | uspto-grants-2016_04 |
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