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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 625446Generated: October 30, 2026

Potassium Carbonate → HCID 64163637, compound

https://huagongshe.com/reaction/625446

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPotassium CarbonateHCID 11430—
ReactantBenzoic acid, 3-mercapto-HCID 95737—
ReactantMethyl 3-(bromomethyl)benzoateHCID 517981—
SolventDimethylformamideHCID 6228—
ProductHCID 64163637HCID 6416363799.2%

Reaction Steps

A mixture of 3-mercaptobenzoic acid (154 mg, 1.00 mmol), methyl 3-(bromomethyl)benzoate (229 mg, 1.00 mmol) and K2CO3 (414 mg, 3.00 mmol) in DMF (1 mL) was stirred for 16 h, then solvent removed. The resulting residue was purified by silica gel chromatography to give 300 mg (90%) of the product.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09301951B2
Source datasetuspto-grants-2016_04
ORD IDord-1f4156f7d2184d38b17222fa41d804a3
Source noteuspto-grants-2016_04