HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 64163637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Benzoic acid, 3-mercapto- | HCID 95737 | — |
| Reactant | Methyl 3-(bromomethyl)benzoate | HCID 517981 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 64163637 | HCID 64163637 | 99.2% |
Reaction Steps
A mixture of 3-mercaptobenzoic acid (154 mg, 1.00 mmol), methyl 3-(bromomethyl)benzoate (229 mg, 1.00 mmol) and K2CO3 (414 mg, 3.00 mmol) in DMF (1 mL) was stirred for 16 h, then solvent removed. The resulting residue was purified by silica gel chromatography to give 300 mg (90%) of the product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09301951B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-1f4156f7d2184d38b17222fa41d804a3 |
| Source note | uspto-grants-2016_04 |