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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 626007Generated: October 29, 2026

5-Bromo-2-nitropyridine → HCID 59191356, compound

https://huagongshe.com/reaction/626007

Reaction equation

Participants

RoleNameHCIDCharge
Reactant5-Bromo-2-nitropyridineHCID 817620—
ReactantHCID 59191405HCID 59191405—
ProductHCID 59191356HCID 59191356103.3%

Reaction Steps

According to the procedure of example 20(a), except substituting 1-fluoro-4-nitro-2-(trifluoromethyl)benzene for 5-bromo-2-nitropyridine (406 mg, 2 mmol), the title compound (220 mg; 38%) was prepared as a white solid, after chromatography on silica gel (gradient cyclohexane/dichloromethane), along with 5-bromo-2-(2-methoxy-4-propylphenoxy)pyridine (238 mg; 37%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS09309179B2
Source datasetuspto-grants-2016_04
ORD IDord-4b0decd2d8864ee484c2daf7b41b5814
Source noteuspto-grants-2016_04