HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Phenyl-1-propanone → 1,1-Bis(4-hydroxyphenyl)-2-phenylbut-1-ene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Phenyl-1-propanone | HCID 7148 | — |
| Reactant | 4,4'-Dihydroxybenzophenone | HCID 69150 | — |
| Product | 1,1-Bis(4-hydroxyphenyl)-2-phenylbut-1-ene | HCID 63059 | 88% |
Reaction Steps
Following general procedure of McMurry reaction as described in example 1, step B, propiophenone (1.9 g, 3.0 eq) was reacted with bis(4-hydroxyphenyl)-methanone (1.0 g, 1.0 eq) to give 1.3 g desired product (88% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309211B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-c780b2b580c84db48e0a5633de90cebd |
| Source note | uspto-grants-2016_04 |