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HRID626153

反应详情

EQUATION

反应方程式

HRID 626153 的结构方程式

REACTANTS

反应物

2
结构：CCC(=O)c1ccccc1
HCID7148

1-Phenylpropan-1-one

C9H10O

结构：CN(C)CCOc1ccc(C(=O)c2ccc(OC3CCCCO3)cc2)nc1
HCID89672891

未命名化合物

PRODUCTS

生成物

1
结构：CCC(=C(c1ccc(O)cc1)c1ccc(OCCN(C)C)cn1)c1ccccc1
HCID78135456

未命名化合物

PROCEDURE

实验过程

Following general procedure of McMurry reaction as described in example 1, step B, (5-(2-(dimethylamino)ethoxy)pyridin-2-yl)(4-(tetrahydro-2H-pyran-2-yloxy) phenyl)methanone (1 eq) was reacted with propiophenone (2 eq) to give the desired product (Z/E=1/1). m/z=389[M+1]+.

WORKUP

后处理

  1. customgeneral procedure of McMurry reaction