HCID 67701573, compound → HCID 67701984, compound

Participants

Reaction Steps

Following the procedure described for N4-[2-(2,6-dichloro-phenyl)-2H-pyrazolo[4,3-c]pyridin-4-yl]-6-methyl-pyrimidine-2,4-diamine, {6-[2-(2,6-dichlorophenyl)-2H-pyrazolo[4,3-c]pyridin-4-ylamino]-2-methyl-pyrimidin-4-yl}-carbamic acid tert-butyl ester was reacted to afford the title compound as a white solid (40 mg, 55% yield). 1H NMR (400 MHz, DMSO-d6): δ 9.93 (s, 1H), 9.16 (s, 1H), 7.90 (d, J=6.4 Hz, 1H), 7.84-7.78 (m, 2H), 7.70 (dd, J=9.0, 7.3 Hz, 1H), 7.57 (s, 1H), 7.12 (d, J=6.4 Hz, 1H), 6.59 (s, 2H), 2.28 (s, 3H). LCMS (Method B): RT=2.90 min, m/z: 386 [M+H+].

Provenance & Evidence