HCID 67701573, compound → HCID 69674857, compound

Participants

Reaction Steps

Following the procedure described for N4-[2-(2,6-dichloro-phenyl)-2H-pyrazolo[4,3-c]pyridin-4-yl]-6-methyl-pyrimidine-2,4-diamine, {6-[2-(2,6-dichlorophenyl)-2H-pyrazolo[4,3-c]pyridin-4-ylamino]-pyrimidin-4-yl}-carbamic acid tert-butyl ester was reacted to afford the title compound as a white solid (148 mg, 50% yield). 1H NMR (400 MHz, DMSO-d6): δ 10.02 (br s, 1H), 9.15 (s, 1H), 8.14 (s, 1H), 7.92 (d, J=6.4 Hz, 1H), 7.84-7.79 (m, 2H), 7.72-7.71 (m, 2H), 7.15 (d, J=6.4 Hz, 1H), 6.71 (br s, 2H). LCMS (Method B): RT=2.85 min, m/z: 372 [M+H+].

Provenance & Evidence