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HRID627213

反应详情

EQUATION

反应方程式

HRID 627213 的结构方程式

REACTANTS

反应物

2
结构：C=CCON[C@H]1CN[C@H](C(N)=O)C(C)=C1C
HCID89851793

未命名化合物

2 次

结构：C=CCON1C(=O)N2C[C@H]1C(C)=C[C@H]2CO[Si](C)(C)C(C)(C)C
HCID89852160

未命名化合物

PRODUCTS

生成物

1
结构：C=CCON1C(=O)N2C[C@H]1C(C)=C(C)[C@H]2C(N)=O
HCID89852291

未命名化合物

收率 66.5%

PROCEDURE

实验过程

The title compound was prepared from (2S,5R)-5-(allyloxyamino)-3,4-dimethyl-1,2,5,6-tetrahydropyridine-2-carboxamide (Intermediate 197, 0.31 g, 1.38 mmol) following the procedure described for Intermediate 13. Silica gel chromatography (0%-70% ethyl acetate/hexanes) afforded the desired product as a white solid (0.23 g, 66.5%).