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HRID627232

反应详情

EQUATION

反应方程式

HRID 627232 的结构方程式

REACTANTS

反应物

3
结构：O=[N+]([O-])c1ccccc1S(=O)(=O)NOCc1ccccc1
HCID9839578

N-(Benzyloxy)-2-nitrobenzenesulfonamide

C13H12N2O5S

结构：C=CCON([C@@H]1C=C(C)[C@@H](CO[Si](C)(C)C(C)(C)C)N(C(=O)OC(C)(C)C)C1)S(=O)(=O)c1ccccc1[N+](=O)[O-]
HCID89852556

未命名化合物

结构：CC(C)(C)OC(=O)N1C[C@@H](O)C(CC[N+](=O)[O-])=C[C@H]1CO[Si](C)(C)C(C)(C)C
HCID89852570

未命名化合物

2 次

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1C[C@H](N(OCc2ccccc2)S(=O)(=O)c2ccccc2[N+](=O)[O-])C(CC[N+](=O)[O-])=C[C@H]1CO[Si](C)(C)C(C)(C)C
HCID89852745

未命名化合物

PROCEDURE

实验过程

The title compound was prepared as a pale yellow oil (5 g, 30%) according to the procedure described for Intermediate 80, from (2S,5S)-tert-butyl 2-((tert-butyldimethylsilyloxy)methyl)-5-hydroxy-4-(2-nitroethyl)-5,6-dihydropyridine-1 (2H)-carboxylate (Intermediate 219, 6.73 g, 16.3 mmol) and N-(benzyloxy)-2-nitrobenzenesulfonamide (7.40 g, 24.00 mmol).