Hydrazine → HCID 178478017, compound

HRID 627990Notes

Reaction equation

HRID 627990 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[CH:25][N:26](C)C)[C:9]([C:11]1[S:24][C:14]2[C:15]3[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=3[O:17][CH2:18][CH2:19][C:13]=2[CH:12]=1)=O.[NH2:29]N>CO>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[C:9]([C:11]2[S:24][C:14]3[C:15]4[CH:23]=[CH:22][CH:21]=[CH:20][C:16]=4[O:17][CH2:18][CH2:19][C:13]=3[CH:12]=2)=[N:29][NH:26][CH:25]=1

Participants

4

Reactant 2

HCID 9321HydrazineHCID 66886006HCID 66886006, compound

Product 1

HCID 178478017HCID 178478017, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

2-(2-Chlorophenyl)-1-(4,5-dihydrobenzo[b]thieno[2,3-d]oxepin-2-yl)-3-(dimethylamino)prop-2-en-1-one was treated with hydrazine in methanol to give 283. MS (ESI) 379.1

Sources & evidence

ORD record
ord-fa0636581cf44ced8e39d00fc196aeab
Source dataset
uspto-grants-2016_04
Patent number
US09309265B2

Reaction notes

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