HRID628102
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
PROCEDURE
实验过程
Following the procedure of Example 15 and General Procedure C, 2-((2,4-difluorophenyl)(methyl)carbamoyl)-4H-thieno[3,2-c]chromene-8-carboxylic acid and dimethylamine were coupled to give 111bp. 1H NMR (400 MHz, CDCl3) δ 7.15-7.31 (m, 3H), 6.82-7.00 (m, 4H), 5.13 (s, 2H), 3.33 (m, 3H), 2.94-3.13 (m, 6H). LCMS (ESI) m/z: 429.1.
WORKUP
后处理
- customto give 111bp