HuagongsheHuagongshe Chemistry Print Report · For research reference only
Morpholine → HCID 44242027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | 8-bromo-N-(2,4-difluorophenyl)-N-methyl-4H-thieno[3,2-c]chromene-2-carboxamide | HCID 57900337 | — |
| Product | HCID 44242027 | HCID 44242027 | — |
Reaction Steps
Following Example 70 and General Procedure D, 8-bromo-N-(2,4-difluorophenyl)-N-methyl-4H-thieno[3,2-c]chromene-2-carboxamide 160bp and morpholine were reacted to give 129bp. 1H NMR (400 MHz, CDCl3) δ: 7.27 (m, 1H), 7.11-7.14 (m, 2H), 6.90-6.98 (m, 3H), 6.75 (s, 1H), 5.09 (s, 2H), 4.04 (m, 2H), 3.38 (s, 3H), 3.32 (m, 2H). LCMS (ESI) m/z: 442.9
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US09309265B2 |
| Source dataset | uspto-grants-2016_04 |
| ORD ID | ord-4019ef011ac047ed9f233e08dadfbe3e |
| Source note | uspto-grants-2016_04 |