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HRID628297

反应详情

EQUATION

反应方程式

HRID 628297 的结构方程式

REACTANTS

反应物

2
结构：CC(=O)O
HCID176

Acetic Acid

C2H4O2

结构：CC(C)(C)OC(=O)NN(C(=O)OC(C)(C)C)c1ccc2c(cc(C(=O)OC(C)(C)C)n2S(=O)(=O)c2ccccc2)n1
HCID118159681

未命名化合物

PRODUCTS

生成物

1
结构：Cc1nnc2ccc3c(cc(C(=O)O)n3S(=O)(=O)c3ccccc3)n12
HCID118159759

未命名化合物

PROCEDURE

实验过程

A solution of di-tert-butyl 1-[2-(tert-butoxycarbonyl)-1-(phenylsulfonyl)-1H-pyrrolo[3,2-b]pyridin-5-yl]hydrazine-1,2-dicarboxylate (0.430 g, 0.730 mmol, from Step 2) in AcOH (7 mL) was heated in the microwave to a temperature of 180° C. for 3 minutes. The solid product was isolated by filtration and air dried, and used without further purification. Yield: (0.106 g, 41%). LCMS (M+H)+: 357.1.

WORKUP

后处理

  1. customThe solid product was isolated by filtration and air
  2. customdried
  3. customused without further purification